DETERMINATION OF SULPHONAMIDE RESIDUES IN HONEYS BY HIGH-PRESSURE LIQUID CHROMATOGRAPHY

publication date: Sep 13, 2013
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Journal of Apicultural Research
Vol. 20 (1) pp.44-48
DOI
          ___
Date
March 1981
Article Title
DETERMINATION OF SULPHONAMIDE RESIDUES IN HONEYS BY HIGH-PRESSURE LIQUID CHROMATOGRAPHY
Author(s)
FLAVIO BELLIARDO
Abstract
A method was developed for determining 3 sulphonamide drug residues in honey at the level of 1 ppm. Residues were extracted with acetone, evaporated to dryness, redissolved in twice-distilled water containing sodium hydroxide, and then directly analysed by reverse-phase high-pressure liquid chromatography. The chromatographic conditions of the analyses and the degradation rates of sulphonamide residues in honey are described and discussed.
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